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    The weight of the title product is 4.80 g (82 % yield), HPLC purity = 99.83%, polymorphic purity is 100% as no detectable polymorph II is observed by X-ray and IR, as shown in Example 3. The HPLC conditions are as follows: Column: SymmetryC 18 , 4.6 x 250 mm λ max 254 nm

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    The weight of the title product is 4.80 g (82 % yield), HPLC purity = 99.83%, polymorphic purity is 100% as no detectable polymorph II is observed by X-ray and IR, as shown in Example 3. The HPLC conditions are as follows: Column: SymmetryC 18 , 4.6 x 250 mm λ max 254 nm

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    2021-7-16 · A generic term for any circumscribed mass of foreign (e.g., lead or viruses) or metabolically inactive materials (e.g., ceroid or MALLORY BODIES), within the cytoplasm or nucleus of a cell. Inclusion bodies are in cells infected with certain filtrable viruses, observed especially in nerve, epithelial, or endothelial cells.

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    When all water was removed from the mixture, the product began slowly to crystallize. The obtained suspension was heated under reflux temperature for 1.5 h, then cooled and filtered. 2.75 g (88 % from N,N-didesmethyl venlafaxine hydrochloride) of pure venlafaxine hydrochloride form I (HPLC: 99.65 area %) were obtained.

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    2018-12-30 · HPLC conditions: aliquots were withdrawn and dissolved in CH 3 CN/H 2 O (40:60). HPLC conditions: Kromasil C4 column, 5 μm, 4.6x150mm, 40 0 C column chamber, flow rate= 1.0 mL/min, 40% CHsCN/60% aqueous (1.OmL 70% HcIO 4 in 1 L H 2 O) isocratic. Percentages reported are at 254 nm.

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    A stock solution of pyrazinamide was prepared in diluent solution (mixture of 50:50% v/v of methanol: HPLC grade water) such that the final concentration was approximately 10 mg/ml. Stock solution of metronidazole (approx 5 mg/ml) is prepared in HPLC grade methanol. The solutions were stored at 4 °C and they were stable for two weeks.

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    2017-8-30 · Antibiotic-resistant in pathogenic bacteria has become a critical public health threat. 1 A major mechanism of antibiotic resistance is microbial degradation of drugs by enzymes such as β-lactamases. Three classes of β-lactamases (A, C, and D) 2 utilize an active-site serine in covalent mechanisms that can be targeted by β-lactamase inhibitors co-formulated with β-lactam drugs.

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    A stock solution of pyrazinamide was prepared in diluent solution (mixture of 50:50% v/v of methanol: HPLC grade water) such that the final concentration was approximately 10 mg/ml. Stock solution of metronidazole (approx 5 mg/ml) is prepared in HPLC grade methanol. The solutions were stored at 4 °C and they were stable for two weeks.

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    2021-5-13 · HPLC buffer A was composed of 0.1% formic acid, and HPLC buffer B was composed of 80% acetonitrile in 0.1% formic acid. Peptides were eluted by a linear gradient from 7 to 36% B over the course of 52 min, after which the column was washed with 95% B and re-equilibrated at 2% B.

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    2017-8-30 · Antibiotic-resistant in pathogenic bacteria has become a critical public health threat. 1 A major mechanism of antibiotic resistance is microbial degradation of drugs by enzymes such as β-lactamases. Three classes of β-lactamases (A, C, and D) 2 utilize an active-site serine in covalent mechanisms that can be targeted by β-lactamase inhibitors co-formulated with β-lactam drugs.

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